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Non-covalent Weak Interactions in Group IV, PT(II) and AU(I) Organometallic Complexes: Synthesis, Structures and Properties

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Non-covalent Weak Interactions in Group IV, PT(II) and AU(I) Organometallic Complexes: Synthesis, Structures and Properties

4.85 84,149 ratings · 5,542 reviews
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Overview: This dissertation, "Non-covalent Weak Interactions in Group IV, PT(II) and AU(I) Organometallic Complexes: Synthesis, Structures and Properties" by Chi-fai, Kui, 居智輝, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. Abstract: Abstract of thesis entitled NON-COVALENT WEAK INTERACTIONS IN GROUP IV, PT(II) AND AU(I) ORGANOMETALLIC COMPLEXES: SYNTHESIS, STRUCTURES AND PROPERTIES Submitted by Kui Chi Fai For the degree of Doctor of Philosophy at The University of Hong Kong in June 2005 The syntheses, characterizations and spectroscopic properties of Group IV, platinum(II) and gold(I) complexes containing cyclometalated ligands are described. The intra-/intermolecular non-covalent interactions and metal-metal interactions in these complexes have been examined by various spectroscopic means. The olefin polymerization catalytic properties of tridentate cyclometalated Group IV complexes, namely [M(C DEGREESN DEGREESO)(CH Ph) ] [HC DEGREESN DEGREESOH = 2-(2'-hyroxyaryl)-6-arylpyridine and 2 2 derivatives; M = Ti, Zr] can be tuned through modifications of the cyclometalating C DEGREESN DEGREESO ligands. A first direct observation of weak intramolecular C-H...F-C contacts in neutral [Zr( C DEGREESN DEGREESO)(CH Ph)] and cationic 2 2 F + - [Zr( C DEGREESN DEGREESO)(CH Ph)] [PhCH B(C F ) ] polyolefin procatalysts is reported here. 2 2 6 5 3 Their molecular structures have been elucidated by X-ray and neutron diffraction crystallography showing the existence of intramolecular C-H...F-C hydrogen bonding, which has also been suggested by NMR measurements. The reactivity of [M(C DEGREESN DEGREESO)(CH Ph) ] [M = Ti, Zr] towards ethylene and 1-hexene polymerization as 2 2 well as ethylene-propylene and ethylene-norbornene copolymerization is described. As the study of attractive interactions between a functionalized ancillary ligand and a growing polymer chain has become a novel concept in olefin polymerization reactions, the results mentioned above can provide strong evidence for designing new catalysts for the precise control of olefin polymerization. The [(R-C DEGREESN DEGREESC)Pt(DMSO)] and [(R-C DEGREESN DEGREESC) Pt (-dppm)] [R-C DEGREESN DEGREESCH = 2 2 2 2,6-di-(2'-naphthyl)pyridine and derivatives] complexes have been prepared. Among the [(R-C DEGREESN DEGREESC) Pt (-dppm)], the crystal lattice of [(C DEGREESN DEGREESC) Pt (-dppm)] has 2 2 2 2 accessible solvent channels (ca. 6.0 4.6 A) and its desolvated form displays a facile and reversible vapoluminescent response upon exposure to VOCs. Comparative PXRD studies showed that desolvation of crystal [(C DEGREESN DEGREESC) Pt (-dppm)] led to a 2 2 more condensed packing of the molecules, which is stabilized by extensive intra-/intermolecular C-H---π and π---π interactions. These extensive weak and reversible interactions could direct the supramolecular assembly of molecular frameworks and fundamentally affect the emission properties of Pt complexes in solid state. The crystal structure and photophysical properties of the [(R-C DEGREESN DEGREESN)PtCl] and [(R-C DEGREESN DEGREESN) Pt (-dppm)](ClO ) (R-C DEGREESN DEGREESNH = 3-(6'-(2"-naphthyl)-2'-pyridyl) 2 2 4 2 isoquinoline and derivatives) are examined. The extending π-conjugated C DEGREESN DEGREESN ligand offers favorable photophysical characteristics compared to 2,2' 6',2"-terpyridine and 6-phenyl-2,2'-bpyridine in planar platinum(II) systems. The high thermal stability of [(R-C DEGREESN DEGREESN)PtCl] reveals that all these materials are suitable for thin film fabrication using chemical vapour deposition. [(C DEGREESN DEGREESC)Au (-dppm)]X [X = Cl, ClO and PF] and 3 2 4 6 [(C DEGREESN DEGREESC) Au (-Ph PC CPPh )] [C DEGREESN DEGREESCH = 2,6-diphenylpyridine] were 2 4 2 2 2 2 prepared using a synthetic strategy based on the directing effect of intramolec

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Chi-Fai Kui
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Chi-Fai Kui is the author of several novels. Originally from the East Coast, they now live in the Midwest with family. In addition to writing, Chi-Fai Kui enjoys gardening, cooking, and reading way past bedtime. Their work often explores the complexities of everyday life and human relationships.

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Mark Carter March 08, 2024
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Christopher Carter February 06, 2025
Masterpiece from start to finish. The prose is exquisite. It’s accessible yet undeniably sophisticated. A true literary gem.
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Excellent, though slightly flawed. It held my rapt attention, even when certain twists were telegraphed. A wonderful companion for a quiet weekend.
Edward Campbell
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It was adequate. It verged on repetitive in the second act. A more concise edit would have served it well. A fair 3 stars.
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Excellent, though slightly flawed. The middle had a deliberate pace, but the climax was phenomenal. Quite impressive overall.
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A very strong entry. The protagonist was compelling, though some subplots felt slightly overshadowed. A wonderful companion for a quiet weekend.
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Exceeded all my expectations. The author orchestrated a breathtaking finale. Truly a work of art. Worth every moment spent reading.
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I was completely blown away. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. An absolute must-read for connoisseurs of the genre.
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Exceeded all my expectations. I became deeply invested in the protagonist's journey. A masterclass in storytelling. I will undoubtedly revisit this masterpiece.
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Masterpiece from start to finish. The author orchestrated a breathtaking finale. Truly a work of art. A true literary gem.
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Exceeded all my expectations. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. A true literary gem.
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Exceeded all my expectations. The author orchestrated a breathtaking finale. Truly a work of art. I will undoubtedly revisit this masterpiece.
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Such a rich narrative. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. An absolute must-read for connoisseurs of the genre.
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I was completely blown away. The prose is exquisite. It’s accessible yet undeniably sophisticated. An effortless 5 stars.
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Daniel Harris
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A profoundly satisfying read. The prose is exquisite. It’s accessible yet undeniably sophisticated. I am now a lifelong fan of this author.
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Honestly one of the most premium reading experiences lately. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. A true literary gem.
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Such a rich narrative. I became deeply invested in the protagonist's journey. A masterclass in storytelling. A true literary gem.
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Honestly one of the most premium reading experiences lately. The prose is exquisite. It’s accessible yet undeniably sophisticated. A true literary gem.
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Such a rich narrative. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. A true literary gem.
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Masterpiece from start to finish. I adored how the story unfolded. It kept me captivated without sacrificing elegance. I am now a lifelong fan of this author.
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Exceeded all my expectations. The prose is exquisite. It’s accessible yet undeniably sophisticated. I will undoubtedly revisit this masterpiece.
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Absolutely brilliant. The author orchestrated a breathtaking finale. Truly a work of art. An absolute must-read for connoisseurs of the genre.
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A decent, if standard, experience. The prose was competent, yet the characters lacked the depth I usually seek. Perhaps more aligned with a different audience's tastes.
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I thoroughly enjoyed the elegance of it. The protagonist was compelling, though some subplots felt slightly overshadowed. I would highly recommend this to discerning readers.
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It was adequate. The prose was competent, yet the characters lacked the depth I usually seek. Perhaps more aligned with a different audience's tastes.
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Christopher Smith March 11, 2025
Masterpiece from start to finish. The prose is exquisite. It’s accessible yet undeniably sophisticated. An effortless 5 stars.
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Linda Reyes April 08, 2025
A profoundly satisfying read. The author orchestrated a breathtaking finale. Truly a work of art. I will undoubtedly revisit this masterpiece.
Nancy Young
Nancy Young January 22, 2025
I was completely blown away. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. I am now a lifelong fan of this author.
Nancy Flores
Nancy Flores August 19, 2025
I thoroughly enjoyed the elegance of it. The protagonist was compelling, though some subplots felt slightly overshadowed. A wonderful companion for a quiet weekend.
Christopher Collins
Christopher Collins June 07, 2025
Exceeded all my expectations. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. A true literary gem.
Michelle Reyes
Michelle Reyes February 03, 2025
Exceeded all my expectations. I became deeply invested in the protagonist's journey. A masterclass in storytelling. An effortless 5 stars.
Michael Hall
Michael Hall March 30, 2024
A very strong entry. The protagonist was compelling, though some subplots felt slightly overshadowed. A wonderful companion for a quiet weekend.
Sharon Martinez
Sharon Martinez January 16, 2024
Exceeded all my expectations. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. A true literary gem.
Eric Moore
Eric Moore April 30, 2025
A profoundly satisfying read. I adored how the story unfolded. It kept me captivated without sacrificing elegance. Worth every moment spent reading.
Michelle Turner
Michelle Turner August 27, 2024
I thoroughly enjoyed the elegance of it. A brilliant concept executed with flair. Just a few pacing choices I would change. A very distinguished novel.
Donald Reyes
Donald Reyes May 23, 2024
Absolutely brilliant. The prose is exquisite. It’s accessible yet undeniably sophisticated. Worth every moment spent reading.
Rebecca Baker
Rebecca Baker February 06, 2024
Absolutely brilliant. I adored how the story unfolded. It kept me captivated without sacrificing elegance. A true literary gem.
Christopher Flores
Christopher Flores March 24, 2024
A profoundly satisfying read. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. An absolute must-read for connoisseurs of the genre.
Linda Nelson
Linda Nelson November 28, 2025
Such a rich narrative. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. I am now a lifelong fan of this author.
Gary Martin
Gary Martin July 03, 2025
Exceeded all my expectations. I became deeply invested in the protagonist's journey. A masterclass in storytelling. An absolute must-read for connoisseurs of the genre.
Eric Flores
Eric Flores September 01, 2025
Not entirely to my refined tastes. It possessed moments of brilliance, but the narrative felt slightly disjointed ultimately. A fair 3 stars.
Kimberly Walker
Kimberly Walker July 30, 2025
Took a moment to build, but the payoff was spectacular. A brilliant concept executed with flair. Just a few pacing choices I would change. A very distinguished novel.
Margaret Gonzalez
Margaret Gonzalez August 11, 2024
I was completely blown away. The author orchestrated a breathtaking finale. Truly a work of art. A true literary gem.
Eric Miller
Eric Miller October 16, 2024
A profoundly satisfying read. The prose is exquisite. It’s accessible yet undeniably sophisticated. I am now a lifelong fan of this author.
Jessica Thompson
Jessica Thompson May 16, 2024
A highly sophisticated read. A brilliant concept executed with flair. Just a few pacing choices I would change. Quite impressive overall.
John Hill
John Hill October 06, 2025
Honestly one of the most premium reading experiences lately. The prose is exquisite. It’s accessible yet undeniably sophisticated. I will undoubtedly revisit this masterpiece.
Ryan Rivera
Ryan Rivera October 05, 2024
I find myself somewhat conflicted. The tempo was somewhat languid, and I found my mind wandering. Not poor, simply average. Perfectly average.
Eric Wilson
Eric Wilson September 06, 2024
I was completely blown away. The prose is exquisite. It’s accessible yet undeniably sophisticated. An absolute must-read for connoisseurs of the genre.
Deborah Walker
Deborah Walker May 10, 2024
Took a moment to build, but the payoff was spectacular. A brilliant concept executed with flair. Just a few pacing choices I would change. A wonderful companion for a quiet weekend.
John Miller
John Miller March 23, 2025
A decent, if standard, experience. It possessed moments of brilliance, but the narrative felt slightly disjointed ultimately. Suitable if your reading queue is empty.
Cynthia Ramirez
Cynthia Ramirez June 27, 2024
Such a rich narrative. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. An absolute must-read for connoisseurs of the genre.
Anthony Thomas
Anthony Thomas August 20, 2025
Masterpiece from start to finish. I adored how the story unfolded. It kept me captivated without sacrificing elegance. Worth every moment spent reading.
Anthony Baker
Anthony Baker October 26, 2024
Honestly one of the most premium reading experiences lately. I became deeply invested in the protagonist's journey. A masterclass in storytelling. Worth every moment spent reading.
Margaret Smith
Margaret Smith February 16, 2025
A highly sophisticated read. It held my rapt attention, even when certain twists were telegraphed. A solid 4 stars from me.
Nicholas Clark
Nicholas Clark September 23, 2024
A profoundly satisfying read. The prose is exquisite. It’s accessible yet undeniably sophisticated. A true literary gem.
Ryan Lee
Ryan Lee November 17, 2025
I was completely blown away. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. Worth every moment spent reading.
Carol Scott
Carol Scott August 24, 2024
A profoundly satisfying read. The author orchestrated a breathtaking finale. Truly a work of art. An effortless 5 stars.
Gary Walker
Gary Walker June 22, 2024
A highly sophisticated read. The middle had a deliberate pace, but the climax was phenomenal. A wonderful companion for a quiet weekend.
Eric Wilson
Eric Wilson September 14, 2025
Absolutely brilliant. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. A true literary gem.
Kimberly Johnson
Kimberly Johnson July 11, 2025
I was completely blown away. The prose is exquisite. It’s accessible yet undeniably sophisticated. An effortless 5 stars.
Mary Scott
Mary Scott December 26, 2024
Such a rich narrative. The author orchestrated a breathtaking finale. Truly a work of art. I am now a lifelong fan of this author.
Christopher Thompson
Christopher Thompson July 12, 2025
Masterpiece from start to finish. I became deeply invested in the protagonist's journey. A masterclass in storytelling. I am now a lifelong fan of this author.
Elizabeth Rodriguez
Elizabeth Rodriguez May 08, 2025
An acceptable diversion. The tempo was somewhat languid, and I found my mind wandering. Not poor, simply average. Suitable if your reading queue is empty.
James King
James King November 11, 2025
I thoroughly enjoyed the elegance of it. Beautiful writing, though I craved slightly more depth in the lore. Still, undeniably engaging. A very distinguished novel.
William Robinson
William Robinson October 10, 2025
Exceeded all my expectations. I became deeply invested in the protagonist's journey. A masterclass in storytelling. An absolute must-read for connoisseurs of the genre.
Laura Flores
Laura Flores March 30, 2024
An acceptable diversion. It verged on repetitive in the second act. A more concise edit would have served it well. A fair 3 stars.
Kenneth Lopez
Kenneth Lopez November 17, 2025
A profoundly satisfying read. The author orchestrated a breathtaking finale. Truly a work of art. Worth every moment spent reading.
Donald White
Donald White November 24, 2024
Honestly one of the most premium reading experiences lately. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. Worth every moment spent reading.
Jessica Ramirez
Jessica Ramirez November 01, 2024
I find myself somewhat conflicted. It verged on repetitive in the second act. A more concise edit would have served it well. A fair 3 stars.
Rebecca Clark
Rebecca Clark July 30, 2025
A decent, if standard, experience. The tempo was somewhat languid, and I found my mind wandering. Not poor, simply average. Perhaps more aligned with a different audience's tastes.
Karen Ramirez
Karen Ramirez August 02, 2024
A highly sophisticated read. The middle had a deliberate pace, but the climax was phenomenal. A solid 4 stars from me.
Stephanie Lee
Stephanie Lee January 03, 2025
Took a moment to build, but the payoff was spectacular. The protagonist was compelling, though some subplots felt slightly overshadowed. Quite impressive overall.
Nicholas Ramirez
Nicholas Ramirez July 01, 2024
Masterpiece from start to finish. The pacing was impeccable and the characters felt incredibly authentic. I was completely immersed. An absolute must-read for connoisseurs of the genre.
Andrew Walker
Andrew Walker October 03, 2024
A highly sophisticated read. The protagonist was compelling, though some subplots felt slightly overshadowed. A very distinguished novel.
Rebecca Baker
Rebecca Baker June 19, 2025
Excellent, though slightly flawed. A brilliant concept executed with flair. Just a few pacing choices I would change. Quite impressive overall.
William Torres
William Torres April 21, 2025
Not entirely to my refined tastes. The prose was competent, yet the characters lacked the depth I usually seek. Unlikely to reread, but a reasonable expenditure of time.
Dorothy Taylor
Dorothy Taylor February 13, 2024
A decent, if standard, experience. It possessed moments of brilliance, but the narrative felt slightly disjointed ultimately. A fair 3 stars.
Daniel Nguyen
Daniel Nguyen September 02, 2024
A profoundly satisfying read. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. A true literary gem.
Kimberly Walker
Kimberly Walker August 28, 2024
A profoundly satisfying read. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. An effortless 5 stars.
Laura  Parker
Laura Parker December 01, 2024
Exceeded all my expectations. The author orchestrated a breathtaking finale. Truly a work of art. An absolute must-read for connoisseurs of the genre.
Michelle Turner
Michelle Turner April 18, 2025
Excellent, though slightly flawed. It held my rapt attention, even when certain twists were telegraphed. A solid 4 stars from me.
Linda Garcia
Linda Garcia June 01, 2024
Masterpiece from start to finish. I became deeply invested in the protagonist's journey. A masterclass in storytelling. A true literary gem.
Andrew Garcia
Andrew Garcia August 28, 2024
I find myself somewhat conflicted. It verged on repetitive in the second act. A more concise edit would have served it well. Suitable if your reading queue is empty.
David Taylor
David Taylor August 21, 2024
A profoundly satisfying read. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. Worth every moment spent reading.
Jacob Jackson
Jacob Jackson October 06, 2025
Exceeded all my expectations. The prose is exquisite. It’s accessible yet undeniably sophisticated. An absolute must-read for connoisseurs of the genre.
Edward Diaz
Edward Diaz December 06, 2024
I was completely blown away. The prose is exquisite. It’s accessible yet undeniably sophisticated. Worth every moment spent reading.
Thomas Diaz
Thomas Diaz September 13, 2025
Honestly one of the most premium reading experiences lately. It strikes a perfect harmony of dialogue and world-building. Every chapter felt necessary. A true literary gem.
Nancy Martin
Nancy Martin June 07, 2024
Absolutely brilliant. I adored how the story unfolded. It kept me captivated without sacrificing elegance. A true literary gem.
Kevin Thompson
Kevin Thompson December 15, 2025
It was adequate. The prose was competent, yet the characters lacked the depth I usually seek. A fair 3 stars.
Ryan Jones
Ryan Jones August 12, 2025
Took a moment to build, but the payoff was spectacular. A brilliant concept executed with flair. Just a few pacing choices I would change. A very distinguished novel.
Lisa Martinez
Lisa Martinez June 03, 2024
I find myself somewhat conflicted. It possessed moments of brilliance, but the narrative felt slightly disjointed ultimately. Suitable if your reading queue is empty.
Sandra Clark
Sandra Clark September 29, 2024
Absolutely brilliant. I adored how the story unfolded. It kept me captivated without sacrificing elegance. An absolute must-read for connoisseurs of the genre.
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